How cheap can radioactive material be? $50? $20? $10? How about $3.99? Went to Walmart (where else) looking for the cheapest ionizing smoke detector they had. Found a $11.99 one and I almost missed this piece of junk on the bottom shelf.
http://i.minus.com/iooRCdj2MjLX.jpgSentry i9040 Smoke Alarm, Walmart price $3.99! Score!
http://i.minus.com/iebvNWkZIH9dy.jpgThis alarm features an ionization sensor designed to detect products of combustion using the ionization technique, it contains 0.9 microcurie of Americium 241, a radioactive material
Bingo that is what we are looking for. A quick tip about smoke detectors, most detectors in the US use Am-241 a radioactive isotope. It might not be as common in other countries and the use of radioactive detectors may be completely outlawed. Am-241 is chosen because it emits (mostly) alpha radiation which is blocked by even a piece of paper or about one inch of air. The packages may say Am-241 on it or it may just was ionizing. There are no radioactive smoke detectors which are optical based so if you see anything on the box about optical detection that is likely not the model you want.
http://i.minus.com/iY8PI0991vfKy.jpgSo there were some kind of clips holding the top on the detector I just broke them by putting a screwdriver between the top and base. Nice thing about $3 smoke detector is the plastic was very cheap and weak. That silver dome is the detection chamber. It is the only part we are interested in. So I just popped the circuit board out and cut the wires.
Safety:
Am-241 is pretty safe as far as radioactive isotopes go but don't be stupid with your health. I recommend you wear gloves and operate on a clean and clear workspace. Throw all the trashed components, your gloves, and any paper towels used to clean up dust into a plastic bag when complete. Since Am-241 is primary an alpha emitted the greatest danger is if you ingest, breath in, or somehow get it into your bloodstream (i.e. cut yourself with a knife that you scrapped some Am-241 onto).
http://i.minus.com/iMWKEnHJ5ehB5.jpgThe backside of the circuit board. Notice the board is covered in wax so if you notice white flakes coming off the board it isn't lethal radioactive material it is just wax. You will notice there are three clips here (first one already destroyed) however that metal cap it actual held in place by the two long solder joints (one to the left of "TP2" and the other just above the arrow in the lower left). You probably could desolder the shield and on a better made model you might have to but this is some cheap junk and after about 3 minutes with a screw driver, needle nose pliers, and some tin snips I ended up with this. There is no exact science to this just use the minimum force necessary you don't want to damage the Am-241 slug.
http://i.minus.com/iSMXogIB9IWHC.jpgThe shield on the right covers the "white stand" which holds the Am-241. The metal foil in the center of the photo is the top conductor. It is attached to the top of the white stand and easy to remove with some pliers. The smaller inner/lower metal foil which is still attached to white stand is the second conductor. When smoke particles enter the space between them they are ionized by the alpha particles emitted by the Am-241 and complete a circuit which trips the alarm. The metal slug in the center of the white stand is what contains the Am-241. We want to remove that as carefully as possible without damaging it. The Am-241 is actually applied in a layer on the surface of the copper colored metal in the indention of the slug. You want to avoid scrapping across that as you could produce dust containing Am-241.
http://i.minus.com/i3cjGPdStGzAB.jpgI found it easiest to rip off the lower foil (needle nose pliers worked great). The slug is wedged into the stand from the backside. You may be able to knock it loose but I found it easier to just cut the cheap white stand down until the slug came free. However you break it out the goal should be to destroy the material around the slug not the slug itself. We are trashing everything else and we want to avoid disturbing the Am-241 on the surface of the slug.
http://i.minus.com/idYSfqiXrPNIx.jpgTada 0.9 microcuries of Am-241 for $3.99 and maybe 10 minutes of work. 1 microcurie scientific samples generally run $50 to $200 so this is quite a deal. It would be a good idea now to clean down your workspace. Dispose of all the other material, used gloves, and cleaning supplies. (in a sealed plastic bag). The Am-241 doesn't need heavy lead shielding but keep out away from children and pets (consumption would be very bad). I stored my sample in a used pill bottle and clearly marked.
DISCLAIMER: Am-241 is relatively safe compared to other isotopes however all radioactive sources this information is provided as educational only and you accept full responsibility for your actions. You are responsible for ensuring that the removal and/or possession of 0.9 microcuries of Am-241 is not prohibited by local law.